Agilent Technologies 1100 Series Instrukcja Obsługi Strona 150
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140 1100 Series Capillary LC System Manual
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Installing the 0.1 - 2.5 ml/min flow capillary kit
1 Switch off the pump module.
2 Disconnect the capillary 01090-87308 between the mixer and the filter.
3 Connect the capillary G1375-87400 to the mixer outlet.
4 Connect the other end of the capillary G1375-87400 to the purge. valve
holder.
5 Install the purge valve holder on the pump head of channel A and fix it with
the screw.
6 Screw the purge valve assembly into the purge valve holder and locate the
outlet and waste.
7 Use the 14 mm wrench to tighten the purge valve assembly.
8 Remove the waste tube from the EMPV and install it to the waste outlet of
the purge valve.
9 Disconnect the capillary on the injection valve (port 1).
10 Connect the capillary G1375-87318 between the purge valve and the
injection valve (port 1).
11 Replace the capillary between the injection valve and the analytical head
with the capillary G1375-87312.
Frequency When the flow rate is higher than 200 µl/min
Tools re quired 4 mm open wrench (8710-1534)
Torque adapter G1315-45003
1/4 - 5/16 inch open wrench (8710-0510)
14 mm wrench (8710-1924)
Parts required Extended flow range kit (G1376-69707)
Purge valve assembly G1311-60009 (supplied in the accessory kit
G1376-68705)
Purge valve holder G1312-23200 (supplied in the accessory kit G1376-68705)
Purge valve holder screw 0515-0175 (supplied in the accessory kit
G1376-68705)
Washer 2190-0586 (supplied in the accessory kit G1376-68705)
- Agilent 1100 Series 1
- Capillary LC System 1
- In This Manual… 3
- Contents 5
- Agilent Technologies 11
- Site Requirements 12
- Bench Space 13
- Environment 13
- Physical Specifications 14
- System Installation Process 16
- Install the Solvent Cabinet 23
- Micro Well-plate Sampler) 26
- Purging the Pump 34
- Inject the Check-out Sample 36
- Procedure 37
- Optimizing Performance 39
- Pump issues 40
- Fused Silica Capillary issues 41
- Sampler issues 42
- Column thermostat issues 42
- DAD issues 42
- Cleaning the Solvent Filters 45
- When to use Alternative Seals 47
- Static Mixer and Filter 50
- How the Function Works 53
- Capillaries and Fittings 55
- Capillary Flow Diagram 56
- Capillaries and Fittings 3 57
- * 2.2 12 5065-9906 61
- * 1.4 7.6 G1375-87313 61
- Fittings and Ferrules 62
- Basic System Troubleshooting 65
- Symptoms: 66
- Poor peak shape 71
- Wandering Detector Baseline 73
- Parts and Materials 75
- Micro Vacuum Degasser 76
- Capillary Pump 79
- Capillary Pump Hydraulic Path 82
- Pump-Head Assembly 84
- Figure 9 Pump head assembly 85
- Capillary pump cover parts 86
- Micro Well-plate Sampler 87
- Thermostat for 1100 Samplers 98
- 5 Parts and Materials 100
- Parts and Materials 5 101
- Vial Trays 104
- Micro Column Switching Valve 107
- Diode Array Detector 111
- DAD - Optical Unit Assembly 113
- Figure 30 Optical Unit Parts 114
- 500 nl Flow Cell 115
- Fan Assembly Parts 117
- Holmium Oxide Filter 118
- Common Parts 120
- Rear panel 121
- Power and Status Light Pipes 122
- Leak Parts 123
- Foam parts 124
- Sheet metal kit 124
- Micro Degasser Accessory Kit 125
- Capillary Pump Accessory Kit 126
- G1316-68725 129
- DAD Accessory Kit 130
- Tabl e 61 Cables overview 131
- Analog Cables 133
- Remote Cables 134
- BCD Cables 140
- Auxiliary Cable 142
- CAN Cable 142
- External Contact Cable 143
- RS-232 Cable Kit 144
- LAN Cables 144
- Options 6 147
- 6Options 152
- Frequency If valve leaks 156
- 9/64 inch hex key 156
- • Disconnect the power cable 157
- • Disconnect capillaries 157
- Features 163
- Performance Specification 163
- Installation of the Flow Cell 166
- ~ 0.3 mm clearance 167
- Replacing or Cleaning Parts 171
- Performance Specifications 175
- 7 Performance Specifications 176
- Performance Specifications 7 177
- Autosampler 179
- Compartment 181
- Safety Information 185
- Operation 186
- Safety Symbols 187
- Lithium Batteries Information 188
- Danish Information: 188
- Radio Interference 189
- Sound Emission 189
- Solvent Information 189
- ' %%(&' 196
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