Agilent Technologies 1100 Series Instrukcja Obsługi Pobierz pdf (Strona 145)

135

Agilent 1100 Series Capillary LC System

System Manual

Agilent Technologies

Options

Extended Flow Range Kit (G1376-69707) 136

0.1 - 2.5 ml/min Flow Capillary Kit (5065-4495) 139

Micro Column Switching Valve G1388A#055 143

500 nl Flow Cell Kit G1315-68714 153

This chapter describes the different options available for the capillary LC

System.

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Agilent 1100 Series 1
Capillary LC System 1
In This Manual… 3
Contents 5
Agilent Technologies 11
Site Requirements 12
Bench Space 13
Environment 13
Physical Specifications 14
System Installation Process 16
Install the Solvent Cabinet 23
Micro Well-plate Sampler) 26
Purging the Pump 34
Inject the Check-out Sample 36
Procedure 37
Optimizing Performance 39
Pump issues 40
Fused Silica Capillary issues 41
Sampler issues 42
Column thermostat issues 42
DAD issues 42
Cleaning the Solvent Filters 45
When to use Alternative Seals 47
Static Mixer and Filter 50
How the Function Works 53
Capillaries and Fittings 55
Capillary Flow Diagram 56
Capillaries and Fittings 3 57
* 2.2 12 5065-9906 61
* 1.4 7.6 G1375-87313 61
Fittings and Ferrules 62
Basic System Troubleshooting 65
Symptoms: 66
Poor peak shape 71
Wandering Detector Baseline 73
Parts and Materials 75
Micro Vacuum Degasser 76
Capillary Pump 79
Capillary Pump Hydraulic Path 82
Pump-Head Assembly 84
Figure 9 Pump head assembly 85
Capillary pump cover parts 86
Micro Well-plate Sampler 87
Thermostat for 1100 Samplers 98
5 Parts and Materials 100
Parts and Materials 5 101
Vial Trays 104
Micro Column Switching Valve 107
Diode Array Detector 111
DAD - Optical Unit Assembly 113
Figure 30 Optical Unit Parts 114
500 nl Flow Cell 115
Fan Assembly Parts 117
Holmium Oxide Filter 118
Common Parts 120
Rear panel 121
Power and Status Light Pipes 122
Leak Parts 123
Foam parts 124
Sheet metal kit 124
Micro Degasser Accessory Kit 125
Capillary Pump Accessory Kit 126
G1316-68725 129
DAD Accessory Kit 130
Tabl e 61 Cables overview 131
Analog Cables 133
Remote Cables 134
BCD Cables 140
Auxiliary Cable 142
CAN Cable 142
External Contact Cable 143
RS-232 Cable Kit 144
LAN Cables 144
Options 6 147
6Options 152
Frequency If valve leaks 156
9/64 inch hex key 156
• Disconnect the power cable 157
• Disconnect capillaries 157
Features 163
Performance Specification 163
Installation of the Flow Cell 166
~ 0.3 mm clearance 167
Replacing or Cleaning Parts 171
Performance Specifications 175
7 Performance Specifications 176
Performance Specifications 7 177
Autosampler 179
Compartment 181
Safety Information 185
Operation 186
Safety Symbols 187
Lithium Batteries Information 188
Danish Information: 188
Radio Interference 189
Sound Emission 189
Solvent Information 189
' %%(&' 196

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